Objective To establish a method to measure acetamiprid in human blood.Methods Acetamiprid in human blood was extracted by dispersive solid phase extraction and analyzed by GC/MS/SIM.Results The concentration of acetamiprid presented a linear range of 0.02μg/mL~2μg/mL(r=0.9997), the recoveries were 76.4%~89.8%, the relative standard deviations were 1.3%~8.3%, the limit of detection was 0.0075μg/ml.Conclusion The method is simple, accurate, easy to use, and suitable for measure of Acetamiprid in human blood.
Key words
Acetamiprid /
dispersive solid phase extraction (DSPE) /
GC/MS/SIM
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Footnotes
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