Determination of acetamiprid in human blood by GC/MS and dispersive solid phase extraction

HOU Hong-an,ZHANG Wei-bing,SU Guo-bao

Forensic Science and Technology ›› 2012, Vol. 37 ›› Issue (2) : 30-31.
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Determination of acetamiprid in human blood by GC/MS and dispersive solid phase extraction

  • HOU Hong-an,ZHANG Wei-bing,SU Guo-bao
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Abstract

Objective To establish a method to measure acetamiprid in human blood.Methods Acetamiprid in human blood was extracted by dispersive solid phase extraction and analyzed by GC/MS/SIM.Results The concentration of acetamiprid presented a linear range of 0.02μg/mL~2μg/mL(r=0.9997), the recoveries were 76.4%~89.8%, the relative standard deviations were 1.3%~8.3%, the limit of detection was 0.0075μg/ml.Conclusion The method is simple, accurate, easy to use, and suitable for measure of Acetamiprid in human blood.

Key words

Acetamiprid / dispersive solid phase extraction (DSPE) / GC/MS/SIM

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HOU Hong-an,ZHANG Wei-bing,SU Guo-bao. Determination of acetamiprid in human blood by GC/MS and dispersive solid phase extraction. Forensic Science and Technology. 2012, 37(2): 30-31

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