On-site Rapid Analysis of Hydroxylimine Based on Surface Acoustic Wave Gas Chromatography

doi:10.16467/j.1008-3650.2019.06.002

Forensic Science and Technology ›› 2019, Vol. 44 ›› Issue (6) : 477-482. DOI: 10.16467/j.1008-3650.2019.06.002

Special for the 13th Five-Year Plan

On-site Rapid Analysis of Hydroxylimine Based on Surface Acoustic Wave Gas Chromatography

ZHU Hongwei¹, WEI Chunsheng², ZHANG Kai³, LIU Jiuling¹, SHAO Jianying¹, LU Yanyan¹, SUN Lin¹, HE Shitang^1,*

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Objective To analyze the volatile and semi-volatile components contained in the residual hydroxylimine manufacture collected on the scene. Methods The hydroxylimine residues were collected, then detected by gas chromatography with surface acoustic wave (GC-SAW), with the related standard materials being determined. The gas chromatography-mass spectrometry (GC-MS) was applied to verify the above determination. Results Both GC-SAW and GC-MS showed that the hydroxylimine residues contains the main component of hydroxylimine plus the raw materials of the synthesized hydroxylamine: 2-chlorobenzonitrile, cyclopentanone and the like. Conclusions GC-SAW can achieve accurate and rapid qualitative analysis of hydroxylimine residues. The method proposed here has the advantages of no pretreatment, fast analysis, and the ability to detect on site, thus bringing forward a new avenue for the rapid detection of precursor chemicals and drugs.

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hydroxylimine / rapid analysis / surface acoustic wave gas chromatography / GC-MS

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ZHU Hongwei, WEI Chunsheng, ZHANG Kai, LIU Jiuling, SHAO Jianying, LU Yanyan, SUN Lin, HE Shitang. On-site Rapid Analysis of Hydroxylimine Based on Surface Acoustic Wave Gas Chromatography. Forensic Science and Technology. 2019, 44(6): 477-482 https://doi.org/10.16467/j.1008-3650.2019.06.002

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Received	Revised	Published
2017-12-12	2018-03-07	2019-12-15
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2019-12-16

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